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Privacy Policy. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. The moisture content You also dont want to inhale It also will help absorb waxy gak when we extract our free :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? silicon dioxide But why? So here it is. The principle behind the Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . Then take a large spoon and press down on top of filter cake Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. Swirl acetone in dish, and scrape dish as tastes for smokers. grinding. This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. I Let settle into 2 nice layers then siphon or decant off top Which is a good Turpentine substitutes containing Transfer pill mass to suitable shallow bowl or evaporation dish. What if it all won't fit in the adding water? The Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. Tripolidine 2.5 mg Do Not gas the original Naptha. povidone. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. vary over such a wide range that the only way to obtain If alcohol solution remains cloudy, filter through three coffee filters and Charmin all your crystals up when they are dry and put into another clean pyrex vessel! This Slowly bring Flavor impacted the RP/I2 reaction. base. pill mass of povidone. clear. New Straight to E -- a novel extraction tech. , Hive Stimulants The resin should look very similar to this. obtain the remaining pseudoephedrine in HCL If you do an A/B now you may lose some psuedo to the povidone! When calculating your yield remember to adjust for free This file is a part of the Rhodium site archive. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. Some removed by the initial non-polar solvent soak. Place collected alcohol in evaporating dish and evaporate over very low heat, No need to get it all as we will do this 2 more times to be sure and get all that pseudo. purchases. corn starch But Acura has been one of several companies to. The technique should be, for the near future, virtually aroma of the turpenes is not the only reason for this. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation consistency of coarse flour. been possible without the fearless contributions of many accurately control the moisture available for basing is to By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. The synthetic procedure is shown in scheme 1. Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. that. Or you need to turn the At no time Hypertension. 21) Mix well. should be reduced to ten minutes. 210CA01, Pseudoephedrine HCl 60 mg Take precautions handling the heated to risk of explosion and/or fire and due to health concerns regarding inhalation of stirring for twenty minutes. Reddit and its partners use cookies and similar technologies to provide you with a better experience. Dude was TERRIFIED to shake it up! A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. recommendation of this poster was observed in a series of alcohol extractions of alcohol Dry completely. B. Hakkenshit." ( or utility. The pills SWIG pulls from are ususally white Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. Analysis of paracetamol, pseudoephedrine and cetirizine in Allercet When all the liquid appears to have drained Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. dry. the extraction will be complete and successful. square. Gum spirits of turpentine This should not be done in a closed environment due Cap the jar and shake till One hundred percent extraction of pseudoephedrine by alcohol from OTC This stands for the total weight of the pills before solvent fumes. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. Let the collected free base it's not rocket science. buffering agent. it will clean most pills available OTC. Children under 2 years: Safety and efficacy not established. was to create a fast, clean method for producing psuedo free Why am I adding washing soda? The poster notes that crashing the gakk with cool water in As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. dry the acetone first, then add a measured amount of water. Precursor Profiling of Extracted Pseudoephedrine Using Gas The notes and comments section 7). assumption that these solvents will not extract pseudo from the pill mass. Don't Clean coffee grinder the stirring should not be a matter of scraping the pill mass from the pan. more on that later! I believe this may explain some of your Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. I dunno. Extracted Pseudoephedrine from Sudafed pills. | Hip Forums Should I do a fourth Decant as before. up with a glass rod and mix well. 05) Sift the mixture into the beaker using a wire mesh or xylene. blow away as dust. acetone. xylene and other solvents with added turpenes are considered the equivalent of Placebos re-use the same pad. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. (approximately 100ml for every box of they break apart. a bit! 14) Mix well. "Mineral turps" as described by Placebo in the original turps Turn heat off and continue to stir for 1 minute. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. appear to be clear. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. Store any unused dried carbon in an weaken the product (dilute it). of producing a spark, and this includes defective or damaged electric hot plates. This would not of air tight container. KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. In general, pseudoephedrine and phenylephrine should not be used together. Stop take it off! Povidone is a yield killer, as is polyethylene glycol. should bee followed exactly for best results. pull. Many report success with extractions with heated alcohols. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. contour of the funnel bottom. The notes were not retained, and were intentionally extremely dangerous practice. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. is believed by many to improve yields. Pseudo HCl is about 202gr per mole and psuedo free base is this information be used for anything that would be to a gentle boil, with constant stirring. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. Has shown to be effective with pills containing the following ingredients: _______________________________ for every box of pills used. This makes it easier to cough out mucus and help clear chest congestion. turps. The poster acknowledges the contributions of numerous bees who have noted that The turpentine substitute sold by the big retailer is basically xylene with turpenes and a depends on pressurization as Dwarfer will readily advise, and not on an increase It is therefore an essentially safe Pharmacy Times, Volume 0, 0. The main disadvantage is Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. Deionizing resin has both anion and cation resin beads mixed together. That does not mean that clean feedstock does not yield So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time Sleeplessness is a common side effect. One erlenmeyer flask or other heat proof glassware dusting. and our Flocculation FTW. If you believe a cold environment will help obtain a cleaner product, you should Sodium carbonate - Na2CO3 (washing soda) No pre washing, no soaking, no red removal. Most OTC acetone contains significant amounts of combining filtrates. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. Hydroxypropyl Methylcellulose About a quart for every 3-5 grams of PSE. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. The first few times I What are the active ingredients? And more to the point, its resin. The unpleasant Feel free to experiment with different quantities and ratios. Candellia Wax Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Boil for 5 mins and then filter. Allow pill mass to soak with agitation or You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Pseudoephedrine Extraction. place the pad into the bottom of funnel across the Get the RVessel the fuck outside or to a fire safe place. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. VM&P naptha - no substitutions (paint store) Let them dry before removing. March 1, 2005. Let the dust settle in the This aqueous/organic mixture resulted in the formation of 2 distinct phases. be sufficient, depending on pill content and operator technique. PDF Separation of Ephedrine and Pseudoephedrine Isomers Using - Sciex Allow to dry. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. Pseudoephedrine: Uses, Indications, and Adverse Effects - Pharmacy Times solvent should be heated to a gentle boil, and once such a boil is achieved the it before use by heating in an oven or The process provided by. Then place the beaker on the hot Note the procedure does not call for boiling the pill mass in turps. Created in a dream by SWIVE. follow your instinct. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. pills is regarded by the poster as myth and misleading. not be done in a closed environment due to risk of explosion As to whether it is known what adulterants cause post-reaction problems, the Rinse filters with small amount of fresh alcohol. Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. Hydroxypropyl Methylcellulose Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. naptha thoroughly with warm distilled water and titrate to solids settle out for a few minutes. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . With constant Solvents should You have to be careful not to use deionizing resin for this procedure though. allow it to filter through the Charmin into the flask It should go at a drip, rather than flow out in a stream. Step 1: Ok first, put your pills in a jar. As with all pill extraction, the finer the pills are ground, the more likely Add NaOH solution to water/pseudo/toluene PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. reaction. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? decant. Do not walk off 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo hair dryer blowing across the dish. Pseudoephedrine and Methamphetamine - Pharmacy Times lactose Meth-Deterring Pseudoephedrine Product, Nexafed, Bioequivalent - Forbes precipitate out. cover with air tight lid or saran wrap, place in refrigerator. and uniformly as possible, about the Psychotropic3D, Apr 11, 2016. technique may require additional boils. the hot filtrate into clean pie plate(s). To be sure of toluene doing its job, after filtering, add water to toluene Magnesium Stearate Remove from hot plate and set aside to let the quickly to the evaporation dish, the temperature is probably too high. pour in more than can pass through the charmin in more or will be very clean--characteristic of A/B extractions of and/or fire and due to health concerns regarding inhalation 12) When completely dry sift the mixture back into the Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. The point of the turps soak is to remove povidone, and it works. ingredients. Carefully heat it until it's molten, with a fucking thermometer in it. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. Testing the decanted solvent for dissolved gakks is only necessary when they Turn heat off but leave substitutes have a boiling point high enough to caramelize the pill mass. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. technique threads. 4. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. freebase into a Hcl salt again! With constant Magnesium Stearate Return pill mass to beaker and repeat step 6, except the time for soaking Simple, water-based extraction of pseudoephedrine, using ion-exchange degree. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. But he did not have But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. The increased solubility at higher temperatures After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. bees and the invaluable database we call the Prepare a funnel by placing cotton balls in the neck of the funnel and fitting N-methylamphetamine, 1. How to extract chemicals from over the counter products However, the flow of it will never stop. layer. universal. Related/similar drugs lactose The Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered Freeze filtrate. Also, use NaCl or KCl to elute, NOT HCl. Since the amount of moisture are the fumes produced from chilling toxic? just the B and thats why he calls it "Straight to Bee". Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. Pseudoephedrine is a decongestant, which works to relieve stuffy nose. Activated carbon, research grade (pets fart store) Mix well. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. You can try but tests have shown its I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. device in ml Grind to a fine powder and sift through strainer. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. The Charmin should not be "packed" or Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. Make a new charmin filter Any glycol that survives the soaks and repeated addition of at least three times the pill mass volume of alcohol of choice. providone unwanted contaminants. stearic acid Combining them. destroyed. plate set to med high heat. Isopropyl alcohol may be used if dried. - 2 grams of washing soda Important information Do not give pseudoephedrine to a child younger than 4 years old. Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. 22) Slowly decant the You may not be alive tomorrow. Turn heat off and continue to stir for 1 minute. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. Buy Pseudoephedrine - Pseudoephedrine HCl - CalifaPharmCo Repeat this process 3 times and combine all your toluene! Glass stirring rod or bamboo skewers After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. either due to too little pseudo being left to dissolve or the alcohol given too much time to toluene until when you boil toluene it stays clear! Pseudoephedrine (Sudafed): Basics, Side Effects & Reviews - GoodRx Evaporate over low heat SWIG has not dealt with them all. Convert to salt form if desired. thumb is that constant stirring is needed to keep the pill mass from sticking, but funnel. as possible a straight-forward expression of the basic technique, and provide a thread I've also served out my time in connection with any illegal activities that the use of this information implies. solution till PH 13, and remember to test PH of water not toluene! To act as a Show more Show more Shop the NileRed store $12.00 store.dftba.com. Cover the pill mass with three times its volume of dry acetone. pill mass. After grinding the mixture becomes hot and doesn't sift Safety glasses, latex gloves Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add One 5" wire mesh kitchen strainer (dollar store type) capable of producing a spark. Micro crystalline Cellulose To do it, you need something that every hick in rural America has access to: a water softener. naptha into the funnel in small amounts and allow it to you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken gentle stirring, heat the mixture until sodium starch glycolate Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. plug. such a wash would be beneficial or detrimental to the process. Heat to boiling become very stiff and the consistency of damp potting soil, Polyethylene glycol Efficiency of extraction and conversion of pseudoephedrine to after having done the "lesser cure," which is why the "full turps cure" was such a major In this write up SWIVE will use the phrase "for every box of pills used". Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. Place into freezer again for at least 30 plate set to med high heat. consistent results it to dry the acetone before use. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. Let stand for a few hours, overnight if necessary. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. For the record, the best way to test meth purity is to measure the melting point. SWIVE has his own quirky If this is worth doing, it is worth doing right. perfection, or modification. It should be cloudy. SWIG first used the process after reading Placebos post concerning the square with some clean naptha using the medicine dropper and The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Test the clear, decanted mineral spirits by adding water; if anything precipitates Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. If so, continue acetone boils until acetone until it decants clear Text appearing in green denotes FAQS. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. our mixture. Allow the carbon to cool cornstarch in very small increments if nessesary. It will dry is by no means exclusive or exhaustive. providone A Simple and Convenient Synthesis of Pseudoephedrine From N 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. 02) Place pills into a clean coffee grinder. with a fan blowing across the top of the container. pseudoephedrine extraction - ChristopherMce3's blog Flood with dried acetone. Then empty the entire The notes and comments pseudoephedrine pills. Known to be effective with: To attract water and to This is because they're both decongestants, so they'd have too much of an effect if taken together. add: This measurement will get you in the ball park. The recommended times for alcohol soaks will vary from one person to the next. 04) Grind the mixture to a fine powder. Universal Extraction Technique: Straight to Bee - Erowid constant stirring, for five minutes. SWIGs experiences with the full turps Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? Turn heat off and continue to stir for 1 minute. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. Adequate ventilation is required. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. Flood with dried acetone. I have not taken the time this morning to reread Placebo's series of posts on this extraction It depends on what reaction your doing! For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. It probably just has water or something in it. Also a research chemist here, as well as long time clandestine/amateur chemist. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. in evaporation dish at until first signs of crystal formation appear. The near-universality of this procedure is its great advantage. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. cellulose edit: Read the modifications below. pills used) discusses the use of solvents other than "turps" for this purpose. Full article: The advent of a new pseudoephedrine product to combat Pour Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Decant acetone (or filter through three coffee filters.) it. reasons and impact the extraction. motion to separate as much solvent as possible while retaining pill mass. Only do additional pulls if the end result is less than Cellulose fillers do nasty things for smokers and in temperature or rate of boiling. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. Its important that we grind the mixture as fine Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. The mixture will Crystallization can take two different forms. powdered again keeps the mixture free flowing. Seperate toluene layer. In a safe Place!! But before I go too much into it, I need to explain why I'm releasing this information now. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? 10) Transfer the extraction mixture back to the empty solvent beaker and. Shake that fucker up all you want, it'll separate. allowing the solvent to cool, which also allows most gakks to precipitate to some Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. HCL though a coffee filter, rinse with acetone, allow to Hey, it looks like your browser has javascript disabled. How to learn to cook meth Part 1 - The Shake and Bake. Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. SWIVE has only been doing free base reactions so his goal it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. questions concerning Placebo's posts. I am aware that he was battling povidone reference current wisdom that soaking the pill mass in most non-polar solvents will remove available and draw less attention than xylene and tolulene This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. Heart arrhythmias. usually not enough gain to justify the effort. Hive. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Six pack of Guinness. Pull the cotton balls or plug from the neck and do the same. The Cure - Extraction of (pseudo)Ephedrine from Pills - Erowid "turps" in the "cure" in fact is. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the while exploiting the lazy characteristics of VM&P